Nanoporous Tungsten Oxide Electrode
Electrochemical oxidation preparing nanoporous tungsten oxide electrode: 1) Treating method for tungsten foil: Firstly cut it into 10mm x 15mm pieces, using waterproof abrasive to polish it, then clean it with acetone, isopropanol, methyl alcohol and deionized water ultrasound cleaning for 15min, blow it with nitrogen gas. 2) Use tungsten foil as anode, Pt foil of 10 x 15mm as counter electrode, put them into electrobath, the distance between two electrodes is 25mm. Then put electrobath in water bath of constant temperature, adjust the bath temperature to control the reaction temperature. The reacting area is 0.88cm2. Adding a certain amount of ready-prepared 1mol/L(NH 4 ) 2 SO 4 solution electrolyte with different concentration of NH 4 F. 3) Clean the ready-prepared WO 3 nanoporous thin film with deionized water, blow-dry with nitrogen gas in the air and put them in muffle furnace, the heating rate is 5℃/min, cool it down to room temperature, then packed it to nanoporous tungst